Spectrocolorimetric and microscopic techniques for the evaluation of plasticized PVC cleaning: a case study applicable to three-dimensional objects at museums

For the validation of a cleaning method in conservation, the examination of the object's surface after the cleaning and the quantification of the cleaning efficiency are significant steps. In this study, several cleaning solutions were tested on a plasticized poly(vinyl chloride) object whose surface was characterized before and after cleaning by optical microscopy and noncontact profilometry. In addition, different methods to quantify the cleaning efficiency based on spectrocolorimetric and microscopic techniques were provided. The results showed that noncontact profilometry supported by optical microscopy and spectrocolorimetry was very useful for the characterization of the plasticized poly(vinyl chloride) surface before and after the cleaning and also for the determination of the cleaners' efficiency.     

A simple approach to neutral atom microscopy

Scanning surfaces using a beam of noncharged atoms or molecules allows for especially nondestructive and low-energy surface imaging, with the potential to obtain new information about surfaces that cannot be easily obtained otherwise. We have developed a new approach, operating with the sample at a close working distance from an aperture, the need for optics to focus the beam is obviated. Compared to more complex approaches, the theoretical performance has no other disadvantage than the short working distance. Resolution of 1.5 μm has been achieved, and submicron resolution appears to be practical. Construction of the microscope and results are presented, including first images done in reflection mode, theory for optimization of the design and avenues for future improvement.     

Integrated electronic transport and thermometry at milliKelvin temperatures and in strong magnetic fields

We fabricated a He-3 immersion cell for transport measurements of semiconductor nanostructures at ultra low temperatures and in strong magnetic fields. We have a new scheme of field-independent thermometry based on quartz tuning fork Helium-3 viscometry which monitors the local temperature of the sample's environment in real time. The operation and measurement circuitry of the quartz viscometer is described in detail. We provide evidence that the temperature of two-dimensional electron gas confined to a GaAs quantum well follows the temperature of the quartz viscometer down to 4 mK.     

Note: The intermodulation lockin analyzer

Nonlinear systems can be probed by driving them with two or more pure tones while measuring the intermodulation products of the drive tones in the response. We describe a digital lockin analyzer which is designed explicitly for this purpose. The analyzer is implemented on a field-programmable gate array, providing speed in analysis, real-time feedback, and stability in operation. The use of the analyzer is demonstrated for intermodulation atomic force microscopy. A generalization of the intermodulation spectral technique to arbitrary drive waveforms is discussed.     

Electrostatic force microscopy of self-assembled peptide structures

In this report electrostatic force microscopy (EFM) is used to study different peptide self-assembled structures such as tubes and particles. It is shown that not only geometrical information can be obtained using EFM, but also information about the composition of different structures. In particular we use EFM to investigate the structures of diphenylalanine peptide tubes, particles, and CSGAITIG peptide particles placed on pre-fabricated SiO(2) surfaces with a backgate. We show that the cavity in the peptide tubes could be due to the presence of water residues. Additionally we show that self-assembled amyloid peptides form spherical solid structures containing the same self-assembled peptide in its interior. In both cases transmission electron microscopy is used to verify these structures. Further, the limitations of the EFM technique are discussed, especially when the observed structures become small compared with the radius of the AFM tip used. Finally, an agreement between the detected signal and the structure of the hollow peptide tubes is demonstrated.     

Image blur and energy broadening effects in XPEEM

We report image blurring and energy broadening effects in energy-filtered XPEEM when illuminating the specimen with soft X-rays at high flux densities. With a flux of 2×10¹³ photons/s, the lateral resolution in XPEEM imaging with either core level or secondary electrons is degraded to more than 50 nm. Fermi level broadening up to several hundred meV and spectral shift to higher kinetic energies are also systematically observed. Simple considerations suggest that these artifacts result from Boersch and Loeffler effects, and that the electron-electron interactions are strongest in the initial part of the microscope optical path. Implications for aberration corrected instruments are discussed.     

Variable space diversity, crossover and mutation in MOEA solving many-objective knapsack problems

In this work, we analyze variable space diversity of Pareto optimal solutions (POS) and study the effectiveness of crossover and mutation operators in evolutionary many-objective optimization. First we examine the diversity of variables in the true POS on many-objective 0/1 knapsack problems with up to 20 items (bits), showing that variables in POS become noticeably diverse as we increase the number of objectives. We also verify the effectiveness of conventional two-point and uniform crossovers, Local Recombination that selects mating parents based on proximity in objective space, and two-point and uniform crossover operators which Controls the maximum number of Crossed Genes (CCG). We use NSGA-II, SPEA2, IBEA _??+? and MSOPS, which adopt different selection methods, and many-objective 0/1 knapsack problems with $n=\{100,250,500,750,\mbox{1,000}\}$ items (bits) and m?=?{2,4,6,8,10} objectives to verify the search performance of each crossover operator. Simulation results reveal that Local Recombination and CCG operators significantly improve search performance especially for NSGA-II and MSOPS, which have high diversity of genes in the population. Also, results show that CCG operators achieve higher search performance than Local Recombination for m?≥?4 objectives and that their effectiveness becomes larger as the number of objectives m increases. In addition, the contribution of CCG and mutation operators for the solutions search is analyzed and discussed.     

Managing Citizen Profiles in the Domain of e-Government: The cPortfolio Project

The provision of support for holistic operations in the scope of a horizontal digital administration requires the fulfillment of a number of previous steps that guarantee the viability of services in the domain. One of these tasks is the proper management of documents. Documents are a key element of any democratic administration and their digital management is a clear pre-requisite for the arrival of digital government. This article tackles how this service can be provided using the support of semantics as a technological cornerstone. The implementation of such a tool is made through the so-called cPortfolio. This platform is deeply discussed and details about its design and implementation are provided. This system is designed to manage both the personal information from the citizen and the documents they possess. Tests on the prototype showed interesting features regarding the simplicity of use and the interoperability support provided to third party agents.     

COACH: COllaborative certificate stAtus CHecking mechanism for VANETs

Vehicular Ad Hoc Networks (VANETs) require mechanisms to authenticate messages, identify valid vehicles, and remove misbehaving vehicles. A public key infrastructure (PKI) can be used to provide these functionalities using digital certificates. However, if a vehicle is no longer trusted, its certificates have to be revoked and this status information has to be made available to other vehicles as soon as possible. In this paper, we propose a collaborative certificate status checking mechanism called COACH to efficiently distribute certificate revocation information in VANETs. In COACH, we embed a hash tree in each standard Certificate Revocation List (CRL). This dual structure is called extended-CRL. A node possessing an extended-CRL can respond to certificate status requests without having to send the complete CRL. Instead, the node can send a short response (less than 1 kB) that fits in a single UDP message. Obviously, the substructures included in the short responses are authenticated. This means that any node possessing an extended-CRL can produce short responses that can be authenticated (including Road Side Units or intermediate vehicles). We also propose an extension to the COACH mechanism called EvCOACH that is more efficient than COACH in scenarios with relatively low revocation rates per CRL validity period. To build EvCOACH, we embed an additional hash chain in the extended-CRL. Finally, by conducting a detailed performance evaluation, COACH and EvCOACH are proved to be reliable, efficient, and scalable.     

Image Compression and Video Segmentation Using Hierarchical Self-Organization

Both image compression based on color quantization and image segmentation are two typical tasks in the field of image processing. Several techniques based on splitting algorithms or cluster analyses have been proposed in the literature. Self-organizing maps have been also applied to these problems, although with some limitations due to the fixed network architecture and the lack of representation in hierarchical relations among data. In this paper, both problems are addressed using growing hierarchical self-organizing models. An advantage of these models is due to the hierarchical architecture, which is more flexible in the adaptation process to input data, reflecting inherent hierarchical relations among data. Comparative results are provided for image compression and image segmentation. Experimental results show that the proposed approach is promising for image processing, and the powerful of the hierarchical information provided by the proposed model.